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U.S.
Patent No. 7,932,095 & UK
Patent No. GB2372102
ICLs
new Real Crystal® IR sample cards provide a conveniently
mounted non-absorbing substrate for qualitative infrared
analysis. They are ideal for liquids, mulls, film casting
from solutions and pyrolosis samples. The 2" x 4"
cards are available with 9.5mm, 15mm and 19mm clear apertures
and they will fit in the universal slide mount of any spectrophotometer.
Space is provided to write on the card to identify the date
of the analysis, the sample identity and the name of the
analyst.
Real
Crystal® IR cards do not exhibit the strong absorbance
peaks found in PTFE and polyethylene sample substrates(see
Fig. 1 & Fig. 2 below). Real Crystal® IR cards are
also unlike screen cards, which allow sample films to break
within a few seconds when the card is placed in the vertical
position and which cut off a significant amount of energy.
Real Crystal® IR cards perform like what these cards
are trying to emulate--real crystals. The alkali halide
sample support substrates (KBr, KCl and NaCl) used in Real
Crystal® IR sample cards transmit in excess of 80% of
the available energy with 15mm and 19mm apertures and in
excess of 70% of the available energy with 9.5mm apertures
(see Figs. 3, 4 & 5 below). In fact, the new Real Crystal®
IR cards perform every bit as well as the crystal blanks
that the 3M® cards sought to emulate. Yet, Real Crystal®
IR cards are inexpensive and disposable because ICL's process
eliminates many of the costly steps required to produce
a crystal blank.
ICL
has prepared these cards with a method that makes them relatively
impervious to atmospheric moisture, thus eliminating storage
issues. And as single use sample substrates, they can be
used with aqueous samples. (See Fig. 6 below).
Real
Crystal® cards are also available with crystal cover
slips. These small square crystal windows can be used with
the 19mm diameter aperture IR cards to sandwich a sample
between the crystal window mounted in the IR card and the
cover slip window to facilitate use of the cards for mulls
and volatile liquid samples.
| Part
No. |
Description |
Price |
| 0000-7095 |
NaCl-Pack
of 25, 9.5mm aperture |
$104.00 |
| 0000-7096 |
KBr-Pack
of 25, 9.5mm aperture |
$129.00 |
| 0000-7097 |
KCl-Pack
of 25, 9.5mm aperture |
$109.00 |
| 0000-7131 |
NaCl-Pack
of 25, 15mm aperture |
$115.00 |
| 0000-7132 |
KBr-Pack
of 25, 15mm aperture |
$139.00 |
| 0000-7133 |
KCl-Pack
of 25, 15mm aperture |
$118.00 |
| 0000-7087 |
NaCl-Pack
of 25, 19mm aperture |
$129.00 |
| 0000-7090 |
KBr-Pack
of 25, 19mm aperture |
$153.00 |
| 0000-7091 |
KCl-Pack
of 25, 19mm aperture |
$134.00 |
| 0000-7092 |
NaCl
Cover Slips, Pack of 25 |
$89.00 |
| 0000-7093 |
KBr
Cover Slips, Pack of 25 |
$103.00 |
| 0000-7094 |
KCl
Cover Slips, Pack of 25 |
$95.00 |
| 0000-7086 |
NaCl
Sample Pack of 5, 9.5mm aperture |
$54.00 |
| 0000-7088 |
KBr
Sample Pack of 5, 9.5mm aperture |
$54.00 |
| 0000-7089 |
KCl
Sample Pack of 5, 9.5mm aperture |
$54.00 |
| 0000-7134 |
NaCl
Sample Pack of 5, 15mm aperture |
$54.00 |
| 0000-7135 |
KBr
Sample Pack of 5, 15mm aperture |
$54.00 |
| 0000-7136 |
KCl
Sample Pack of 5, 15mm aperture |
$54.00 |
| 0000-7098 |
NaCl
Sample Pack of 5, 19mm aperture |
$54.00 |
| 0000-7099 |
KBr
Sample Pack of 5, 19mm aperture |
$54.00 |
| 0000-7100 |
KCI
Sample Pack of 5, 19mm aperture |
$54.00 |
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FIGURE
1: PTFE
3M sample card absorbance spectrum.
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FIGURE
2: Polyethylene
3M sample card absorbance spectrum.
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FIGURE
3: Spectrum
of NaCl crystal sample support
mounted in 19mm aperture Real Crystal® IR Card.
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FIGURE
4: Spectrum
of KCl crystal sample support
mounted in 19mm aperture Real Crystal® IR Card.
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FIGURE
5: Spectrum
of KBr crystal sample support
mounted in 19mm aperture Real Crystal® IR Card.
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FIGURE
6: Absorbance
spectrum of polyvinyl alcohol film cast
from aqueous solution on a KBr Real Crystal® IR
Card.
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