Dia-Braze™ High Pressure Diamond Horizontal ATR

 




The Dia-Braze™ features a single reflection diamond optical element which is brazed into tungsten carbide as its sampling stage. The anvil that compresses the sample onto the sampling stage is sapphire. This combination of extremely hard and durable materials enables application of extremely high pressures on the sample using the bridge style pressure applicator, which has a built in pressure control mechanism. By enhancing contact between the optic and the diamond optical sampling stage, optimum optical contact is assured.
Once optimum optical contact has been achieved, no increase in absorbance intensity is possible and maximum sensitivity is achieved. By assuring optimum contact, the Dia-Braze™ enables control over reproducibility of results from sample to sample.
The Dia-Braze™ is available with several very useful options. There are seven anvil options (see product description below) which include the standard sapphire anvil, volatiles cover, view through, flow through, pellet anvil, reactive anvil, flat anvil, and 2 grooved anvils. A germanium top plate is available for very strongly absorbing samples. An optional heated top plate with diamond optics can heat samples to 200°C. A reaction vessel for pressures up to 3000 psi at 200°C is available for flow through and static sampling. A wire holder top plate set with two (2) grooved anvils is available for the study of coated wires. A specular reflection top plate is available for micro reflectance samples, very highly absorbing samples and carbon black containing polymers.

Part No. Description
0015-6925 Dia-Braze™ single reflection HATR with brazed diamond optic sample stage, sapphire anvil with calibrated pressure applicator, KRS-5 lenses, Constant Purge™, pellet anvil and volatiles cover
0015-6929 Dia-Braze™ complete with heated top plate. Same as 0015 6925, but includes 30 volt DC heated top plate and combination temperature controller DC power supply and RS-232 computer interface, for 115v
0015-6930 Same as 0015-6929, but for 220v
0015-7469 Heated diamond top plate only, with temperature controller as in 0015-6929
0015-6926 Germanium top plate only (used with 0015-6939)
0015-7472 Wire Holder Diamond Top plate, complete with 2 grooved anvils (0015-6937 & 0015-6938), for precise positioning of coated wires
0015-6941 Reaction Cell -- contact ICL for details
0015-7470 View through pressure applicator bridge, 4X lens system and built in illuminator, non-rotating sapphire anvil is viewing window
0015-7471 Flow through anvil, 28 microliter volume, up to 1000 psi, 1/16" OD flow tubes, can be used with heated top plate 0015-6929 and with unheated top plate
0015-6935 Volatiles cover
0015-6933 Sapphire Anvil, self leveling
0015-6939 Stainless Steel anvil, for use with Ge top plate and with fibers and fine wires
0015-6934 Pellet anvil with concave surface to hold polymer pellets
0015-6938 Grooved anvil (wide), for coatings on wires
0015-6937 Grooved anvil (narrow) for coatings on wires
0015-6936 Reactive Sample Anvil with "o" ring seals dry samples loaded in glove box to keep sample dry