For making thin films from polymers that can be dissolved into solutions, the Roto-Film™ is an excellent alternative. Films are spin cast on a rapidly turning platen designed to hold standard aluminum weighing dishes, which are disposable. The edges of the weighing dish can be cut off to make a flat highly reflective surface that can be placed into a specular reflection accessory for analysis or the film can simply be peeled off the bottom of the weighing dish. Alternatively, films can be cast on a polished aluminum concave platen, on a Real Crystal® IR Card or on a KBr window. For most polymers, the film is complete within 60 seconds. If the film is cast on a KBr window, the window is simply mounted in a spectrophotometer for analysis. Films cast on polished platens are removed simply by contacting tape with the edge of the film and then pulling the film off of the platen.
The
Roto-Film produces films which are extraordinarily
consistent from film to film. The accessory employs a programmable
positive feedback micro-processor controlled motion controller
and a programmable timer to precisely reproduce cycle time,
rotation speed and ramp up and ramp down from run to run.
Films
cast by rotational casting on KBr windows, Real Crystal®
IR Cards or which are analyzed by specular reflection are
free of interference fringes. Rotational casting produces
films with radial symmetry, which means that the film molecules
radiate from a central point like spokes on a wheel rather
than exhibiting the monodirectional orientation typical
of extruded films. Extruded films will exhibit different
absorbance peak intensities depending upon how the film
is oriented when it is placed in a spectrophotometer, but
radially symmetric films cast on the Roto-Film will
exhibit the same peak intensities regardless of how the
film is oriented when it is placed in the spectrophotometer. An anti-static block is recommended to aid in film removal.
| Part
No. |
Description |
| 0014-6031 |
Roto-Film
film maker with disposable film casting platens, permanent
polished aluminum flat platen, crystal casting platen,
digital microprocessor motion controller, programmable
cycle timer, 110 v, 60Hz |
| 0014-6909 |
Roto-Film
for use in countries with 220v, 50 Hz power, same as
above unit with CE marked transformer & country
specific power cord & plug set |
| 0014-6273 |
Concave
platen |
| 0014-6276 |
Microscope
slide platen |
| 0014-7451 |
Real
Crystal® IR Card platen |
| 0014-6275 |
Static dissipation tool for film removal |
|