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This
heated cell can be configured as a gas cell (Fig. 2) or
for vaporizing samples that are normally solids or liquids
at room temperature. Configured for gas sampling, the cell
incorporates 2 valves, an inlet and an outlet, that enable
flowing gas samples through the cell.
In its solid and liquid
vaporization configuration, the cell has an outlet needle
valve from which a vacuum can be pulled and two (2) sample
inlets. One
inlet is a needle septa injection port on the top of the
cell which is similar to the type used in gas chromatography.
There is a second inlet in the form of a side port for inserting
solid samples, which also doubles as the thermocouple port.
Using the side port eliminates the need to recheck vacuum
seals whenever the cell is opened to insert solid samples.
The 250w heating jacket extends over the end of the cell
so that both the cell body and the optics are heated, and
allows operation at temperatures up to 200°C. Condensation
on the optics is minimized by heating them to the same temperature
as the sample chamber. A type J iron constantan thermocouple
is provided with plugs which are compatible with the optional
temperature controller. The cell body is type 304 stainless
steel and an assortment of seals is provided silicon
rubber, viton and PTFE.
Cells
are factory pretested for vacuum leaks using dummy windows
and then new windows are shipped with the cell. The cell
comes standard with 47 x 6mm KCl windows. The clear aperture
is 39mm. Other window materials are available. An optional
high stability temperature controller with RS-232 computer
interface and Windows® compatible software is available.
The temperature controller (see
description) has ramp and soak cycles that can be programmed
either on the keypad or from a PC using the provided software
and the RS232 interface.
| Part
No. |
Description |
Price |
| 0007-5546 |
10cm
vapor gas multi-sampler with sheathed Iron Constantan
304SS type J thermocouple, 115v, 250w heater system,
Swagelok® vacuum valve, thermocouple port, injection
port heatable to 200 degrees C, heated windows to prevent
fogging, KCl windows, 303SS body.
|
$2289.00 |
| 0007-5547 |
Same
as 0007-5546 with KBr windows. |
$2359.00 |
| 0007-8032 |
10cm
vapor gas multi-sampler with sheathed iron Constantan
304SS type J thermocouple, 220v, 250w heater system,
Swagelok® vacuum valve, thermocouple port, injection
port heatable to 200 degrees C, heated windows to prevent
fogging, KCI windows, 303SS body. |
$2369.00 |
| 0007-8033 |
Same
as 0007-8032 with KBr windows |
$2449.00 |
| 0017-5548 |
High Stability PID Temperature Controller for 0007-5546,
115v, RS-232 interface and Windows® based software
for PC control, digital readout, keypad or PC programmable
for ramp up, ramp down, set point, and soak (dwell)
time as well as for temperature settings, digital readouts
of all parameters. |
$1799.00 |
| 0017-4804 |
Same
as 0017-5548 but 230v, CE marked. |
$1899.00 |
| 0008-5162 |
Cylindrical Cell Holder for 0007-5546 and 0007-5547 |
$159.00
|
| 0007-7405 |
10cm
heated gas cell, KCl windows, two Swagelok® valves,
type J Iron Constantan thermocouple, 115v, 250w heater
jacket. Requires temperature controller (Part no. 0017-5548)
and cell mount (Part No. 0008-5162) |
$2299.00 |
| 0007-7406 |
Same as 0007-7405 with KBr windows. |
$2369.00
|
| 0007-8034 |
10cm
heated gas cell, KCI windows, two Swagelok® valves,
type J Iron Constantan thermocouple, 220v, 250w heater
jacket. Requires temperature controller (0017-4804)
and cell mount (0008-5162). |
$2499.00
|
| 0007-8035 |
Same
as 0007-8034 with KBr windows |
$2579.00
|
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